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Herein we show that heating 2D Ti 3 C 2 in air resulted in TiO 2 nanocrystals on thin sheets of disordered graphitic carbon structure that can handle extremely high cycling rates when tested as anodes in lithium ion batteries. Oxidation of 2D Ti 3 C 2 in either CO 2 or pressurized water also resulted in TiO 2 /C hybrid structure. Similarly, other hybrids can be produced, as we show here for Nb 2 O 5 /C from 2D Nb 2 C.
